Spectrometric Identification of Organic Compounds

By: Silverstein, Robert MContributor(s): Webster, Francis XMaterial type: TextTextPublication details: New Delhi: John Wiley, 2009Edition: 6th edDescription: xiv, 482 p. : ill. ; 29 cmISBN: 9788126509720; 8126509724Subject(s): Spectrum analysis | Organic compounds--Spectra | Spectrometer | Organic compounds | Chemistry, Analytic--QualitativeDDC classification: 547
Contents:
Chapter 1. Mass Spectrometry. -- 1.1 Introduction. -- 1.2 Instrumentation. -- 1.3 Ionization Methods. -- 1.4 Mass Analyzers. -- 1.5 Interpretation of El Mass Spectra. -- 1.6 Mass Spectra of Some Chemical Classes. -- Chapter 2. Infrared Spectrometry. -- 2.1 Introduction. -- 2.2 Theory. -- 2.3 Instrumentation. -- 2.4 Sample Handling. -- 2.5 Interpretations of Spectra. -- 2.6 Characteristic Group Absorption of Organic Molecules. -- Chapter 3. Proton Magnetic Resonance Spectrometry. -- 3.1 Introduction. -- 3.2 Theory. -- 3.3 Instrumentation and Sample Handling. -- 3.4 Chemical Shift. -- 3.5 Spin Coupling, Multiplets, Spin Systems. -- 3.6 Protons on Oxygen, Nitrogen, and Sulfur Atoms. Exchangeable Protons. -- 3.7 Coupling of Protons to Other Important Nuclei (F19, E, P31, Si29, and C13. -- 3.8 Chemical Shift Equivalence. -- 3.9 Magnetic Equivalence (Spin-Coupling Equivalence). -- 3.10 AMX, ABX, and ABC Rigid Systems with Three Coupling Constants. -- 3.11 Confirmationally Mobile, Open-Chain Systems. Virtual Coupling. -- 3.12 Chirality. -- 3.13 Vicinal and Geminal Coupling. -- 3.14 Low-Range Coupling. -- 3.15 Selective Spin Decoupling. Double Resonance. -- 3.16 Nuclear Overhauser Effect, Difference Spectrometry, 1H 1H Proximity Through Space. -- Chapter 4. Carbon-13 NMR Spectrometry. -- 4.1 Introduction. -- 4.2 Theory. -- 4.3 Interpretation of a Simple C13 Spectrum: Diethyl Phthalate. -- 4.4 Quantitative C13 Analysis. -- 4.5 Chemical Shift Equivalence. -- 4.6 DEPT. -- 4.7 Chemical Classes and Chemical Shifts. -- Chapter 5. Correlation NMR Spectrometry; 2-D NMR. -- 5.1 Introduction. -- 5.2 Theory. -- 5.3 Correlation Spectrometry. -- 5.4 Ipsenol: H1-H1 COSY. -- 5.5 Caryophyllene Oxide. -- 5.6 C13-C13 Correlations: Inadequate. -- 5.7 Lactose. -- 5.8 Relayed Coherence Transfer: TOCSY. -- 5.9 HMQC -- TOCSY. -- 5.10 ROESY. -- 5.11 VGSE. -- 5.12 Gradient Field NMR. -- Chapter 6. NMR Spectrometry of Other Important Spin 1/2 Nuclei. -- 6.1 Introduction. -- 6.2 N15 Nuclear Magnetic Resonance. -- 6.3 F19 Nuclear Magnetic Resonance. -- 6.4 Si29 Nuclear Magnetic Resonance. -- 6.5 P31 Nuclear Magnetic Resonance. -- 6.6 Conclusion. -- Chapter 7. Solved Problems. -- 7.1 Introduction. -- Chapter 8. Assigned Problems. -- 8.1 Introduction. -- Problems.
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Item type Current library Call number Copy number Status Notes Date due Barcode Item holds
General Books General Books Central Library, Sikkim University
General Book Section
547 SIL/S (Browse shelf(Opens below)) C2 Available 052334
General Books Science Library General Books Science Library Science Library, Sikkim University
547 SIL/S (Browse shelf(Opens below)) C1 Available Books For SU Science Library P04820
Total holds: 0

Chapter 1. Mass Spectrometry. --
1.1 Introduction. --
1.2 Instrumentation. --
1.3 Ionization Methods. --
1.4 Mass Analyzers. --
1.5 Interpretation of El Mass Spectra. --
1.6 Mass Spectra of Some Chemical Classes. --
Chapter 2. Infrared Spectrometry. --
2.1 Introduction. --
2.2 Theory. --
2.3 Instrumentation. --
2.4 Sample Handling. --
2.5 Interpretations of Spectra. --
2.6 Characteristic Group Absorption of Organic Molecules. --
Chapter 3. Proton Magnetic Resonance Spectrometry. --
3.1 Introduction. --
3.2 Theory. --
3.3 Instrumentation and Sample Handling. --
3.4 Chemical Shift. --
3.5 Spin Coupling, Multiplets, Spin Systems. --
3.6 Protons on Oxygen, Nitrogen, and Sulfur Atoms. Exchangeable Protons. --
3.7 Coupling of Protons to Other Important Nuclei (F19, E, P31, Si29, and C13. --
3.8 Chemical Shift Equivalence. --
3.9 Magnetic Equivalence (Spin-Coupling Equivalence). --
3.10 AMX, ABX, and ABC Rigid Systems with Three Coupling Constants. --
3.11 Confirmationally Mobile, Open-Chain Systems. Virtual Coupling. --
3.12 Chirality. --
3.13 Vicinal and Geminal Coupling. --
3.14 Low-Range Coupling. --
3.15 Selective Spin Decoupling. Double Resonance. --
3.16 Nuclear Overhauser Effect, Difference Spectrometry, 1H 1H Proximity Through Space. --
Chapter 4. Carbon-13 NMR Spectrometry. --
4.1 Introduction. --
4.2 Theory. --
4.3 Interpretation of a Simple C13 Spectrum: Diethyl Phthalate. --
4.4 Quantitative C13 Analysis. --
4.5 Chemical Shift Equivalence. --
4.6 DEPT. --
4.7 Chemical Classes and Chemical Shifts. --
Chapter 5. Correlation NMR Spectrometry; 2-D NMR. --
5.1 Introduction. --
5.2 Theory. --
5.3 Correlation Spectrometry. --
5.4 Ipsenol: H1-H1 COSY. --
5.5 Caryophyllene Oxide. --
5.6 C13-C13 Correlations: Inadequate. --
5.7 Lactose. --
5.8 Relayed Coherence Transfer: TOCSY. --
5.9 HMQC --
TOCSY. --
5.10 ROESY. --
5.11 VGSE. --
5.12 Gradient Field NMR. --
Chapter 6. NMR Spectrometry of Other Important Spin 1/2 Nuclei. --
6.1 Introduction. --
6.2 N15 Nuclear Magnetic Resonance. --
6.3 F19 Nuclear Magnetic Resonance. --
6.4 Si29 Nuclear Magnetic Resonance. --
6.5 P31 Nuclear Magnetic Resonance. --
6.6 Conclusion. --
Chapter 7. Solved Problems. --
7.1 Introduction. --
Chapter 8. Assigned Problems. --
8.1 Introduction. --
Problems.

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