Silverstein, Robert M <br/><br/>
Spectrometric Identification of Organic Compounds 

 - 6th ed. 
 - New Delhi:  John Wiley,  2009. 
 - xiv, 482 p. :  ill. ;  29 cm. 
<br/><br/>Chapter 1. Mass Spectrometry. --<br/>1.1 Introduction. --<br/>1.2 Instrumentation. --<br/>1.3 Ionization Methods. --<br/>1.4 Mass Analyzers. --<br/>1.5 Interpretation of El Mass Spectra. --<br/>1.6 Mass Spectra of Some Chemical Classes. --<br/>Chapter 2. Infrared Spectrometry. --<br/>2.1 Introduction. --<br/>2.2 Theory. --<br/>2.3 Instrumentation. --<br/>2.4 Sample Handling. --<br/>2.5 Interpretations of Spectra. --<br/>2.6 Characteristic Group Absorption of Organic Molecules. --<br/>Chapter 3. Proton Magnetic Resonance Spectrometry. --<br/>3.1 Introduction. --<br/>3.2 Theory. --<br/>3.3 Instrumentation and Sample Handling. --<br/>3.4 Chemical Shift. --<br/>3.5 Spin Coupling, Multiplets, Spin Systems. --<br/>3.6 Protons on Oxygen, Nitrogen, and Sulfur Atoms. Exchangeable Protons. --<br/>3.7 Coupling of Protons to Other Important Nuclei (F19, E, P31, Si29, and C13. --<br/>3.8 Chemical Shift Equivalence. --<br/>3.9 Magnetic Equivalence (Spin-Coupling Equivalence). --<br/>3.10 AMX, ABX, and ABC Rigid Systems with Three Coupling Constants. --<br/>3.11 Confirmationally Mobile, Open-Chain Systems. Virtual Coupling. --<br/>3.12 Chirality. --<br/>3.13 Vicinal and Geminal Coupling. --<br/>3.14 Low-Range Coupling. --<br/>3.15 Selective Spin Decoupling. Double Resonance. --<br/>3.16 Nuclear Overhauser Effect, Difference Spectrometry, 1H 1H Proximity Through Space. --<br/>Chapter 4. Carbon-13 NMR Spectrometry. --<br/>4.1 Introduction. --<br/>4.2 Theory. --<br/>4.3 Interpretation of a Simple C13 Spectrum: Diethyl Phthalate. --<br/>4.4 Quantitative C13 Analysis. --<br/>4.5 Chemical Shift Equivalence. --<br/>4.6 DEPT. --<br/>4.7 Chemical Classes and Chemical Shifts. --<br/>Chapter 5. Correlation NMR Spectrometry; 2-D NMR. --<br/>5.1 Introduction. --<br/>5.2 Theory. --<br/>5.3 Correlation Spectrometry. --<br/>5.4 Ipsenol: H1-H1 COSY. --<br/>5.5 Caryophyllene Oxide. --<br/>5.6 C13-C13 Correlations: Inadequate. --<br/>5.7 Lactose. --<br/>5.8 Relayed Coherence Transfer: TOCSY. --<br/>5.9 HMQC --<br/>TOCSY. --<br/>5.10 ROESY. --<br/>5.11 VGSE. --<br/>5.12 Gradient Field NMR. --<br/>Chapter 6. NMR Spectrometry of Other Important Spin 1/2 Nuclei. --<br/>6.1 Introduction. --<br/>6.2 N15 Nuclear Magnetic Resonance. --<br/>6.3 F19 Nuclear Magnetic Resonance. --<br/>6.4 Si29 Nuclear Magnetic Resonance. --<br/>6.5 P31 Nuclear Magnetic Resonance. --<br/>6.6 Conclusion. --<br/>Chapter 7. Solved Problems. --<br/>7.1 Introduction. --<br/>Chapter 8. Assigned Problems. --<br/>8.1 Introduction. --<br/>Problems. 
<br/><br/><label>ISBN: </label>9788126509720  8126509724 
<br/><br/><label>Subjects--Topical Terms: </label><br/>Spectrum analysis<br/>Organic compounds--Spectra<br/>Spectrometer<br/>Organic compounds<br/>Chemistry, Analytic--Qualitative
<br/><br/><label>Dewey Class. No.: </label>547  / SIL/S